Choose the thermo scientific icap rq icpms for a complete. Yag 266 nm laser ablation load coil torch cones inductively coupled plasma interface vacuum pumps quadrupole lens mass spectrometer. In order to comply with the requirements described above for 21 cfr part 11 compliance, the thermo scienti. It is known and used for its ability to detect metals and several nonmetals in liquid samples at very low concentrations. The thermo scientific icap q icpms was validated for use against revision 5. Powerful interference reduction for reliable and accurate quantification. Unfortunately as from july we have been having problems with performance checks. The icap q icpms has been developed with groundbreaking technology to enable advanced highperformance analysis combined with total reliability and ultraflexibility. Inductively coupled plasma mass spectroscopy icpms. The icap q is easier to use, simpler to maintain, and delivers more performance than any other system giving you total confidence in your results, whether you perform routine analyses or stateoftheart research. Analysis of dissolved trace elements in aqueous solutions by icp.
For information about the operating procedures for the. Drinking water compliance monitoring using us epa method. Our product line consists of autosamplers, microflow pfa nebulizers, concentric nebulizers, apex desolvation nebulizers, pc3 peltier coolers, mp2 micro peristaltic pumps, fast solutions, application solutions and consumables. It describes the modes of operation and principle hardware components of your icap q mass spectrometer and provides stepbystep instructions for cleaning and maintaining your instrument. Elemental scientific specializes in inert and highsensitivity sample introduction systems for icpaes and icpms elemental analysis. Connect peripheral devices in minutes, thanks to an openaccess, sample introduction area. Your icp works by ionising the elements and passing these elements into the ms. Icpoes has much higher tolerance for tds up to 30%. Ergonomically designed quadrupole icp ms with smallest bench space availableinnovat.
Thermo scientific icap 7000 series icpoes genecraft labs. The icap q icp ms has been developed with groundbreaking technology to enable advanced highperformance analysis combined with total reliability and ultraflexibility. This icap q operating manual contains precautionary statements that can prevent personal injury, instrument damage, and loss of data if properly followed. Pdf on apr 7, 2015, martin tanner and others published icptof by tofwerk, status march 2015 find, read and cite all the research you need on researchgate. These ions are then separated and detected by the mass spectrometer. Elemental imaging and petrovolcanological applications of an. The thermo scientific icap tq icpms is the solution to futureproofing your laboratory.
Delivering triple quadrupole technology, the thermo scientific icap tqs icp ms is a highperformance icp ms for ultratrace quantification of trace elements in a variety of challenging matrices related to the semiconductor industry. The vacuum pump edwards is enclosed in the noise reduction cabinet, under your mass spectrometer icap q icp ms. Inductively coupled plasma mass spectrometry icp ms. The entry level icap qa icp ms provides multielemental analytical capabilities without the need to invest in collision cell technology. An innovative multistage peltiercooled desolvation system combined in series with a helical eptfe fluoropolymer membrane desolvator gives maximum icpms signal while simultaneously reading the lowest ratios of oxide. As shown in figure 1, icpms consists of an ion source icp, a sampling interface, ion lens, a mass spectrophotometer and a detector. The coupling of the ics5000 ion chromatographic system with the icap q icpms has been shown to be a powerful tool for the detection of low concentrations of arsenic species in fruit juices. Antivirus and malware prevention in goanywhere mft. Thermo scientific icap q icpms industrial area of thessaloniki, block no. Mar 02, 2016 your icp works by ionising the elements and passing these elements into the ms. The vacuum pump edwards is enclosed in the noise reduction cabinet, under your mass spectrometer icap q icpms. Overview to scale the picture below is a simulation at scale of the thermo icap q icp ms mass spectrometer system, installed on a ionbench ms mass spec benchtable. Icap is an open protocol and allows any server or application provider to implement it.
The ms relies on the charge of the ions to separate the masses and assumes that all ions are singly charged. Autotuning fails, mass calibration fails, cross calibration fails. The interface is the region where ions generated in the plasma are transferred from atmospheric pressure to the vacuum region and introduced to the mass spectrometer as an ion beam. Therefore, no security changes to the existing network are likely. Userinspired hardware and software combine in the thermo scientific icap rq icpms to deliver maximized productivity and robustness.
Determination of trace elements in waters and wastes. Routine 247 workhorse for laboratories upgrading from aa or the icap qc icp ms is configured for high icp oes. Easytouse system developed to support ultralow detection limits, and has improved interference removal capabilities. Inductively coupled plasma mass spectrometry icpms. Icpmass spectrometry the 30minute guide to icpms a worthy member of the inorganic analysis team for nearly 30 years, inductively coupled plasmamass spectrometry icpms has been gaining favor with laboratories around the world as the instrument of choice for performing trace metal analysis. View online or download thermo scientific icap rq icpms preinstallation requirements manual. Interface thermo fisher scientific icap q operating manual pn 1288090, revision b 37. Inductively coupled plasmamass spectrometry icpms is a powerful tool for analyzing trace metals in environmental samples.
We have had an icap q icp ms installed for the last couple of months. The reliability, analytical performance and ease of use needed to meet the demands of the. Qtegra software platform, there is no need for additional software. Ionbench with the thermo icap q icpms mass spectrometer. Pdf inductively coupled plasma mass spectrometry icp ms. The esi prepfast 2 autodilution system is fully integrated for seamless.
Trace element speciation using ic icp ms analysis of lithiumion battery degradation products duration. The coupling of the ics5000 ion chromatographic system with the icap q icpms has been shown to be a powerful tool for the detection of low concentrations of. With bench height, open access to the icap q icpms sample introduction system, specialized sample introduction systems e. Elemental scientific specializes in inert and highsensitivity sample introduction systems for icp aes and icp ms elemental analysis. Novel qcell technology for inference removal in icpms. Overview to scale the picture below is a simulation at scale of the thermo icap q icpms mass spectrometer system, installed on a ionbench ms mass spec benchtable. Instrument control is used by the manager to switch on, optimize and calibrate the icap q instrument.
To prevent viruses, malware and other malicious content from entering your organization, goanywhere mft can integrate with antivirus solutions using the standard icap protocol. Inductively coupled plasmamass spectrometry icp ms is a powerful tool for analyzing trace metals in environmental samples. Users can switch between single and triple quadrupole modes within a single multielement experiment. To run a measurement the appropriate experiment configuration has to be loaded.
There is a container on the work bench of the icpms lab room 204a designated for. Agilents marketleading inductively coupled plasma mass spectrometry icpms systems provide flexible and reliable solutions for elemental analysis. The bench surface should ideally be 80 to 85 cm above the floor. Each pillar is carefully optimized to deliver simplicity, productivity, efficiency and quality in your laboratory. When a new file is uploaded to goanywhere mft, the file contents can be sent to the antivirus software for scanning. Manuals picture pn description quantity 1288090 icap q operating manual 1 1288021 icap q preinstallation requirements guide 1 table 11. Inductively coupled plasma mass spectrometry icpms with. Single quadrupole inductively coupled plasma mass spectrometry sqicpms thermo fisher scientific us. Low cost per sample operator time is freed up with simple workflows and a minimal number of steps per task. Icap is easy to implement since it leverages apache code. Thermo scientific icap q software manual pn 1288010, revision b 11 chapter 1 using this manual this icap q software manual introduces the software suite qtegra and describes the configuration and operation of the icap q instrument with qtegra. The thermo scientific qtegra intelligent scientific data solution isds is a software platform built on four pillars.
As shown in figure 1, icp ms consists of an ion source icp, a sampling interface, ion lens, a mass spectrophotometer and a detector. Inductively coupled plasma mass spectrometry wikipedia. This dual mode technology enables advanced flexibility for optimization, quantification and internal standardization. Currently, one of the greatest challenges in water analysis is the monitoring of multiple metals in a large number of samples with varying concentrations. A large range of elements can be detected using an icpms, which are summarized in figure 1 below. Technical data icap rq 2channel instrument the table summarizes the most important technical data of the icap rq icpms systems. Workflow, data management, scalability and compliance. Thermo scientific icap q icpms rob henry and julian wills, thermo fisher scientific, germany application note 43127 key words icap q, us epa method 200. The determination of major and trace elements in milk using icpq. Instrument control overview thermo scientific icap q software manual pn 1288010, revision b 25.
Multielement determination in food samples using the thermo. Without reaction finder with reaction finder select select the analytes to be measured select. Thermo scientific icp techniques, reduces training requirements and makes the addition of a sqicpms into your lab a simple process. If you try to attach a file format that is not accepted, you will see this message. In meeting this, agilent has developed a range of advanced applications for its portfolio of highproductivity instruments that deliver the sensitivity needed across a wide dynamic range. Simplicity and easeofuse work in concert to streamline workflows and achieve rightfirsttime results.
The icap q gc icp ms coupling kit incorporates a unique dual mode sample introduction system for the simultaneous introduction of a liquid in parallel to the gc outlet. Elemental scientific designs and produces a full range of automation and sample introduction systems for the determination of trace element concentrations in liquid samples by inductively coupled plasma instrumentation. Thermo scientific ics5000 was coupled to the icap q for subsequent speciation determinations. A large range of elements can be detected using an icp ms, which are summarized in figure 1 below. Jul 12, 2012 lothar rottmann from thermo scientific gives us a detailed tour of their new icap q icpms system that has been designed from the ground up. Faster method development for improved productivity. The icap tqs icp ms system from thermo scientific offers high performance icp ms for ultratrace quantification of trace elements in a variety of semiconductors. The ion source, icp is an ideal ionization source for mass spectrometry, and can ionize over 90% of many elements. Br43207 thermo scientific icap q brochure pragolab. Placing the ms system thermo fisher scientific icap q preinstallation requirements guide pn 1288020, revision a 25. Autodilution higher throughput, lower maintenance and autodilution reduce time and cost.
Elemental scientific improve icpms lab results with. Ergonomically designed quadrupole icpms with smallest bench space availableinnovat. What do i do if i start uploading documents and cant complete the upload because the system cannot accommodate them. Drinking water compliance monitoring using us epa method 200. Daily performance check in icpms scientist solutions. The operating condition of the icp ms and the specifications of each configuration are reported in table 1. Experience a dramatically different icpms for total reliability with maximized uptime and a dramatically simplified workflow with the thermo scienti. Thermo scientific qtegra intelligent scientific data solution. Parameter specification value instrument dimensions icap rq icpms length. To demonstrate how simultaneous determination of all elements of interest in a wide range of food samples. See the respective chapters of the manual for details and additional instrument properties. Analysis of pharmaceutical products for their elemental impurities.
The installation of your icap q icp ms cannot be scheduled until this form is completed and returned to the above address. Our icpms and icpqqq instruments offer the highest matrix tolerance and unmatched interference removal, delivering fast, accurate and consistently reproducible results even for trace metals. Our extensive product line contains sample introduction devices for all models of. The icap 7000 series icpoes offers three models, all of which enable global regulatory compliance, in a wide range of fields, and each instrument is designed to suit the specific throughput requirements of a variety of users. Elements detectable by icp ms analysis perkinelmer.
Impurities are a prevalent issue in the semiconductor industry, particularly semiconductor wafer production. Analysis of nanoparticles using the icap q icp ms kutscher, daniel. Miscellaneous pictures pn description quantity 1600550 inline water filter 5. The operating condition of the icpms and the specifications of each configuration are reported in. Tubing for sampler has been changed, torch has been changed, cones and lenses cleaned. Minimal installation and bench space requirements ensure any laboratory will benefit from this technology. Inductively coupled plasma mass spectrometry icpms is a type of mass spectrometry that uses an inductively coupled plasma to ionize the sample.
The thermo scientific icap tq icpms is the solution to futureproofing. The icap q instrument is designed to be placed on a bench with its rear panel against a wall. Overall it is a cheaper option if the elements do not need lower detection limit like icpms does. The get ready feature takes your icap rq icpms from standby to.
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